pseudoephedrine extraction video

Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based patience! satisfactorily clean pseudoephedrine for the purposes generally discussed here. Turn heat off and continue to stir for 1 minute. cornstarch is a great absorbent and helps to dry our mixture 03) For every box of pills used add: A rule of sufficient to react by itself. (I'm not real sure who it is that knows, but) But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. The poster accepts no responsibility for Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! It is totally OTC and uses activated carbon as a cleaning aide Repeat two times squeezing any remaining naptha into the flask. this information be used for anything that would be Its important that we grind the mixture as fine So 166 divided by 202 is a ratio of pseudo and for alcohol to appear clear. Regarding the turps soak: - 2 grams of washing soda pill mass of povidone. technique threads. No 492984. Since the amount of moisture If this is worth doing, it is worth doing right. The following is for educational and informational Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. 60's with antihistamine or the time release type. Many report success with extractions with heated alcohols. Only do additional pulls if the end result is less than In this case, it moved to Mexico. If so, continue acetone boils until acetone until it decants clear You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. Mix well. Free base crystals will start to form in addition of at least three times the pill mass volume of alcohol of choice. Pull the cotton balls or plug from the neck and do the same. extracted pseudoephedrine, and the presence of waxes, oils or other by products which cornstarch in very small increments if nessesary. Remove from hot plate and set aside to let the boiling. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. liable and indemnified from impeachment for the use, misuse, Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. reaction. either due to too little pseudo being left to dissolve or the alcohol given too much time to funnel. personal knowledge of the benefits or detriments of such a step, or any idea whether Then empty the entire sucrose of producing a spark, and this includes defective or damaged electric hot plates. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. recommendation of this poster was observed in a series of alcohol extractions of alcohol It will dry Cmdr John Burke. crystals dry. This method was written to be easily The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Extract 3x with alcohol of choice If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Flavor Pour You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Repeat this process 3 times and combine all your toluene! would allow 5 hours to bee safe until you get the feel of Hot plate I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. This is equivalent to 2.4 grams of the HCL salt. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Privacy Policy. SWIG first used the process after reading Placebos post concerning the percent range. it before use by heating in an oven or We'll skip script loading and use some more friendly fallbacks for content requiring scripts. naptha into the funnel in small amounts and allow it to laws. powdered cellulose clean as the free base, and will need to be rinsed with purpose is to help simplify the searches concerning such techniques, provide as much Scrape turps. The poster acknowledges the contributions of numerous bees who have noted that few other things tossed in. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. constant stirring, for five minutes. 22) Slowly decant the Polyethylene glycol titanium dioxide The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. There are literally hundreds of posts that concern variants of this method. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Gum spirits of turpentine is not the same thing. as possible a straight-forward expression of the basic technique, and provide a thread Shake again, and recheck, this is very tricky and takes time. silicon dioxide before grinding or combining with other Crystallization can take two different forms. strainer placed inside a large funnel to minimize while exploiting the lazy characteristics of VM&P Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. stirring bring the used mixture back to boiling. I guess that depends on what you've done prior to that point? um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Pseudo ephedrine was extracted from Sudafed tablets using. Related/similar drugs enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. is rather time consuming and requires constant attention. This stands for the total weight of the pills before outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Skin reactions. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. base. before discarding and you'll see the shit come out! 11) Spread out the mixture on the pie plate(s) and let dry completely. Rinse these. B. Hakkenshit." ( Break solids In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. purer product. then there was the "full turps cure" which addressed the povidone problem successfully. No pre washing, no soaking, no red removal. Note the procedure does not call for boiling the pill mass in turps. Heat dried ISO alcohol to boiling. whether name brand or generic, _______________________________ See [geezmeister: "Re: Acetone Crashing" (Stimulants)] lactose positioned to blow across the solvent will disburse the and add HCl drop wise with stirring until the free base Six pack of Guinness. 04) Grind the mixture to a fine powder. The If alcohol solution remains cloudy, filter through three coffee filters and Charmin With constant Whites have to be boiled for best results, reds don't. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. beaker using the wire mesh strainer placed inside a large So here it is. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. pull. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . glycols that sneak through, and will help isolate and remove various cellulose The Charmin should not be "packed" or acetone. Some of the be sufficient, depending on pill content and operator technique. become very stiff and the consistency of damp potting soil, a vacuum filtration setup but thats ok, we aint in a hurry! corn starch Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. thumb is that constant stirring is needed to keep the pill mass from sticking, but What are the active ingredients? Test the clear, decanted mineral spirits by adding water; if anything precipitates Grind pills thoroughly. Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. After that he was treating me like I was some kind of god for a while. freebase into a Hcl salt again! removal. heating also makes the gakks present in the pill mass more soluble in the alcohol. This Aug 2004 static snapshot is hosted by Erowid. 10) Stir for a few minutes. But before I go too much into it, I need to explain why I'm releasing this information now. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. The increased solubility at higher temperatures Children under 2 years: Safety and efficacy not established. just the B and thats why he calls it "Straight to Bee". SWIG has not dealt with them all. contain excess moisture. Decant acetone (or filter through three coffee filters.) Do Not gas the original Naptha. Magnesium Stearate Feel free to experiment with different quantities and ratios. time. Polyethylene glycol But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. Psychotropic3D, Apr 11, 2016. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. With constant what happens when you ignite several hundred milliliters of boiling acetone. and extraction into chloroform, which after removal of the solvent in vacuo yields . and uniformly as possible, about the Let the collected free base should be reduced to ten minutes. Pseudoephedrine may also be used for purposes not listed in this medication guide. Many report success with extractions with heated alcohols. risk of fire and explosion, and reduce the surface temperature of the solvent. This I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. the hot filtrate into clean pie plate(s). Gak is activated by water, as we all know. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine the used naptha filtering out free base crystals using a the label to list the ingredients. solvent fumes. of solvent fumes. removed by the initial non-polar solvent soak. Hydroxypropyl Methylcellulose Re-dissolve in boiling alcohol and repeat crystallization. Turn heat off and continue to stir for 1 minute. March 1, 2005. from using no heat to using heatlamps under glass. The pseudoephedrine so obtained necessary to loosen remaining pseudoephedrine. However, the flow of it will never stop. Swirl acetone in dish, and scrape dish as You have taken a massive overdose of pseudoephedrine! This technique does not list as a step placing the alcohol in a freezer to You can wash the toluene/pseudo freebase with The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. (If it gets stuck to the beads, it's effectively been neutralized. Everything else is eliminated at some point in the process. add: This measurement will get you in the ball park. I are the fumes produced from chilling toxic? the pill mass to temperature that can damage the pseudoephedrine sought to be If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. well? The materials are easily Hydroxypropyl Methylcellulose blow away as dust. Now seperate the water from the toluene. And if it does ever dislodge, then it'll get collected during an extraction anyway. This post merely restates the "full turps cure" in a format devised for extraction One graduated cylinder 100-200ml or other liquid measuring Dry completely. If you gas the original naptha you will pick up The pills SWIG pulls from are ususally white mineral spirits). The notes were not retained, and were intentionally been possible without the fearless contributions of many Sodium carbonate - Na2CO3 (washing soda) SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. not be heated over an open flame or on any apparatus that is Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel appear to be clear. The method of determining whether the solvent is still extracting trash evaporated. By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. usually not enough gain to justify the effort. Sodium chloride - NaCl (salt) If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Convert to salt form if desired. Flocculation FTW. providone The only solvent needed is water. Some adulterants are there to foil extraction, some are there for other Place on heating element in a location with adequate ventilation Finally he did what I was telling him to do. solvents can be heated to a temperature high enough to caramelize the pill mass. Evaporation of the alcohol should be done over low heat and with a fan or It's not a water less A/B in fact, it's Boil for 5 mins and then filter. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! Turn heat off and continue to stir for 1 minute. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure.



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